O²-(N^α-acetyl-L-phenylalanine)methyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O²-(N^α-acetyl-L-phenylalanine)methyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate
• CAS No.: 340728-91-8
• Molecular Formula: C₁₆H₂₂N₄O₅
• Molecular Weight: 350.374

Synonyms:O²-(N^α-acetyl-L-phenylalanine)methyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate

Chemical Property of O²-(N^α-acetyl-L-phenylalanine)methyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate

Chemical Property:

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Technology Process of O²-(N^α-acetyl-L-phenylalanine)methyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate

There total 2 articles about O²-(N^α-acetyl-L-phenylalanine)methyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(S)-2-acetylamino-3-phenylpropanoic acid (2018-61-3) + O2-(chloromethyl)-1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate (340728-86-1,960231-74-7) → O2-(Nα-acetyl-L-phenylalanine)methyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate (340728-91-8)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/S0040-4039(01)00263-5

Reference yield:

O2-methylthiomethyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate (340728-85-0) → O2-(Nα-acetyl-L-phenylalanine)methyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate (340728-91-8)

Guidance literature:

Multi-step reaction with 2 steps

1: SO₂Cl₂ / CH₂Cl₂ / 0.67 h

2: 60 percent / Cs₂CO₃ / dimethylformamide / 20 °C

With sulfuryl dichloride; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(01)00263-5

upstream raw materials:

(S)-2-acetylamino-3-phenylpropanoic acid

O²-(chloromethyl)-1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate

O²-methylthiomethyl 1-(pyrrolidin-1-yl)diazen-1-ium-1,2-diolate

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