C₂₇H₂₈ClN₅O₃

Base Information

Chemical Name:C₂₇H₂₈ClN₅O₃
CAS No.:1364680-52-3
Molecular Formula:C₂₇H₂₈ClN₅O₃
Molecular Weight:506.004
Hs Code.:

C<sub>27</sub>H<sub>28</sub>ClN<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₇H₂₈ClN₅O₃

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Chemical Property of C₂₇H₂₈ClN₅O₃

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Technology Process of C₂₇H₂₈ClN₅O₃

There total 5 articles about C₂₇H₂₈ClN₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1364717-85-0
C₃₃H₄₂ClN₅O₄Si

: 1364680-52-3
C₂₇H₂₈ClN₅O₃

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1364717-17-8
C₂₂H₂₉ClN₄O₂Si

: 1364680-52-3
C₂₇H₂₈ClN₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N,N,N,-tetramethylethylenediamine; lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 60 °C / Inert atmosphere

1.2: 0.5 h / 60 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With N,N,N,N,-tetramethylethylenediamine; caesium carbonate; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 177219-28-2
1-[4-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-1-methyl-ethylamine

: 1364680-52-3
C₂₇H₂₈ClN₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / water; ethyl acetate / 0.67 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

3: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With tetrabutyl ammonium fluoride; sodium hydrogencarbonate; caesium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;