4-[(4-chloropyrimidin-2-yl)amino]benzenesulphonyl chloride hydrochloride

Base Information

• Chemical Name: 4-[(4-chloropyrimidin-2-yl)amino]benzenesulphonyl chloride hydrochloride
• CAS No.: 1037622-38-0
• Molecular Formula: C₁₀H₇Cl₂N₃O₂S*ClH
• Molecular Weight: 340.617

Synonyms:4-[(4-chloropyrimidin-2-yl)amino]benzenesulphonyl chloride hydrochloride

Chemical Property of 4-[(4-chloropyrimidin-2-yl)amino]benzenesulphonyl chloride hydrochloride

Chemical Property:

Purity/Quality:

≥95% ^*data from raw suppliers

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-[(4-chloropyrimidin-2-yl)amino]benzenesulphonyl chloride hydrochloride

There total 1 articles about 4-[(4-chloropyrimidin-2-yl)amino]benzenesulphonyl chloride hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-N-phenylpyrimidin-2-amine (52057-92-8) → 4-[(4-chloropyrimidin-2-yl)amino]benzenesulphonyl chloride hydrochloride (1037622-38-0)

Guidance literature:

With chlorosulfonic acid; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

4-(2-pyrrolidin-1-ylethylamino)piperidine-1-carboxylic acid tert-butyl ester (919834-57-4) + 4-[(4-chloropyrimidin-2-yl)amino]benzenesulphonyl chloride hydrochloride (1037622-38-0) → 4-[[4-(4-Chloropyrimidin-2-ylamino)benzenesulphonyl]-(2-pyrrolidin-1-ylethyl)amino]piperidine-1-carboxylic acid tert-butyl ester (919836-60-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 18h;

upstream raw materials:

4-chloro-N-phenylpyrimidin-2-amine

Downstream raw materials:

4-[[4-(4-Chloropyrimidin-2-ylamino)benzenesulphonyl]-(2-pyrrolidin-1-ylethyl)amino]piperidine-1-carboxylic acid tert-butyl ester

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