3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide

Base Information

Chemical Name:3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide
CAS No.:960526-58-3
Molecular Formula:C₂₁H₁₉BrF₂N₄OS
Molecular Weight:493.375
Hs Code.:

Synonyms:3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide

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Chemical Property of 3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide

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Technology Process of 3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide

There total 6 articles about 3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1,3-diamino-2,2-difluoropropane hydrochloride

: 960526-56-1
3-[4-(3-bromophenyl)-2,5-dithioxo-1,3-thiazolidin-4-yl]-N,N-dimethylbenzamide

: 960526-58-3
3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide

Guidance literature:: With triethylamine; In ethanol; at 70 ℃; for 12h;

Reference yield: 100.0%

: 960526-58-3
3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide

Guidance literature:

Reference yield:

: 960526-83-4
C₂₀H₂₅BrN₂O₂S

: 960526-58-3
3-[8-(3-bromophenyl)-3,3-difluoro-6-thioxo-2,3,4,6,7,8-hexahydroimidazo[1,5-a]pyrimidin-8-yl]-N,N-dimethylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; methanol / diethyl ether / 0.5 h

2: dichloromethane / 2 h / 25 °C

3: potassium tert-butylate / tetrahydrofuran / 0.5 h / -78 - 20 °C

4: triethylamine / ethanol / 12 h / 70 °C

With hydrogenchloride; methanol; potassium tert-butylate; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;