C₃₆H₄₇O₈P

Base Information

• Chemical Name: C₃₆H₄₇O₈P
• CAS No.: 1282618-52-3
• Molecular Formula: C₃₆H₄₇O₈P
• Molecular Weight: 638.738
• Mol file: 1282618-52-3.mol

Synonyms:C₃₆H₄₇O₈P

Chemical Property of C₃₆H₄₇O₈P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₄₇O₈P

There total 5 articles about C₃₆H₄₇O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[4-(3'-benzyl-4'-hydroxy-benzyl)-3,5-dimethylphenoxy]methylphosphonic acid (852949-30-5) + iodomethyl pivaloate (53064-79-2) → C36H47O8P (1282618-52-3)

Guidance literature:

[4-(3'-benzyl-4'-hydroxy-benzyl)-3,5-dimethylphenoxy]methylphosphonic acid; With N,N-diethyl-N-isopropylamine; In acetonitrile; at 20 - 40 ℃;

iodomethyl pivaloate; In acetonitrile; at 40 ℃;

Reference yield:

3,5-Dimethylphenol (108-68-9,50356-23-5) → C36H47O8P (1282618-52-3)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sodium hydroxide / water / 1.5 h / Large scale

1.2: 4 °C / Large scale

2.1: caesium carbonate / dimethyl sulfoxide / 8 h / 50 - 60 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / -1 °C

4.1: potassium iodide; chloro-trimethyl-silane / acetonitrile / 50 °C

5.1: N,N-diethyl-N-isopropylamine / acetonitrile / 20 - 40 °C

5.2: 40 °C

With chloro-trimethyl-silane; N,N-diethyl-N-isopropylamine; caesium carbonate; trifluoroacetic acid; potassium iodide; sodium hydroxide; In dichloromethane; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

2,6-dimethyl-4-hydroxybenzyl alcohol (28636-93-3) → C36H47O8P (1282618-52-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: caesium carbonate / dimethyl sulfoxide / 8 h / 50 - 60 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / -1 °C

3.1: potassium iodide; chloro-trimethyl-silane / acetonitrile / 50 °C

4.1: N,N-diethyl-N-isopropylamine / acetonitrile / 20 - 40 °C

4.2: 40 °C

With chloro-trimethyl-silane; N,N-diethyl-N-isopropylamine; caesium carbonate; trifluoroacetic acid; potassium iodide; In dichloromethane; dimethyl sulfoxide; acetonitrile;

upstream raw materials:

3,5-Dimethylphenol

2,6-dimethyl-4-hydroxybenzyl alcohol

C₁₆H₂₇O₅P

[4-(3'-benzyl-4'-hydroxy-benzyl)-3,5-dimethylphenoxy]methylphosphonic acid