(5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione

Base Information

Chemical Name:(5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione
CAS No.:1186579-83-8
Molecular Formula:C₂₆H₁₉N₃O₅
Molecular Weight:453.454
Hs Code.:

Synonyms:(5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione

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Chemical Property of (5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione

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Technology Process of (5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione

There total 1 articles about (5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1186579-60-1
(5R,11aS)-2-(4-benzoic acid ethyl ester)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione

: 1186579-83-8
(5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran;
DOI:10.1039/b902319d

Reference yield: 45.0%

: 189209-27-6
tert-butyl N-[2-[2-[2-[2-[2-(2-aminoethoxy)ethoxy]ethoxy] ethoxy]ethoxy]ethyl]carbamate

: 1186579-83-8
(5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione

: 1186579-84-9
C₄₃H₅₃N₅O₁₁

Guidance literature:: (5R,11aS)-2-(4-benzoic acid)-5-(3-hydroxyphenyl)-6H-1,2,3,5,11,11a-hexahydroimidazo[1,5-b]-β-carboline-1,3-dione; With O-(1,2-dihydro-2-oxo-1-pyridyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In N,N-dimethyl-formamide; for 18h;

tert-butyl N-[2-[2-[2-[2-[2-(2-aminoethoxy)ethoxy]ethoxy] ethoxy]ethoxy]ethyl]carbamate; In N,N-dimethyl-formamide; for 72h;
DOI:10.1039/b902319d