5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine

Base Information

Chemical Name:5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine
CAS No.:108561-09-7
Molecular Formula:C₂₅H₂₃NO₃
Molecular Weight:385.463
Hs Code.:

5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenz<b,g>azocine

Synonyms:5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine

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Chemical Property of 5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine

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Technology Process of 5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine

There total 3 articles about 5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 108561-08-6
5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-(R,S)-5,7-dihydroxy-5,7-dimethyldibenzazocine

: 108561-09-7
5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine

Guidance literature:: With phosgene; In dichloromethane; toluene; at 0 - 25 ℃;
DOI:10.1021/jo00390a005

Reference yield: 21.0%

: 108561-08-6
5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-(R,S)-5,7-dihydroxy-5,7-dimethyldibenzazocine

: 108561-10-0
2-acetyl-2'-carbomethoxy-2-isopropenyltriphenylamine

: 108561-09-7
5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine

Guidance literature:: With aluminum oxide; In chloroform; for 6h; Heating;
DOI:10.1021/jo00390a005

Reference yield:

: 34069-90-4
2,2',2-Nitrilotrisbenzoesaeure-trimethylester

: 108561-09-7
5,6,7,12-tetrahydro-N-(2-carbomethoxyphenyl)-5-hydroxy-5-methyl-7-methylenedibenzazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 64.7 percent / tetrahydrofuran; diethyl ether / 6 h / 50 °C

2: 21 percent / Al₂O₃ / CHCl₃ / 6 h / Heating

With aluminum oxide; In tetrahydrofuran; diethyl ether; chloroform;
DOI:10.1021/jo00390a005