trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol

Base Information

Chemical Name:trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol
CAS No.:115819-61-9
Molecular Formula:C₁₉H₃₂O
Molecular Weight:276.462
Hs Code.:

Synonyms:trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol

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Chemical Property of trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol

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Technology Process of trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol

There total 5 articles about trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 115819-60-8
trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane

: 115819-61-9
trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol

Guidance literature:: With hydrogen fluoride; In acetonitrile; for 6h; Ambient temperature;

Reference yield:

: 109263-23-2,115889-37-7
3-{(1R,2S)-2-[1-(tert-Butyl-dimethyl-silanyloxy)-allyl]-1-methyl-cyclohexyl}-propionaldehyde

: 115819-61-9
trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / tetrahydrofuran / 0.5 h / Ambient temperature

2: 74 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 85 percent / butyl-lithium / tetrahydrofuran / -78 deg C, 1 h, room temperature, 1 h

4: 54 percent / thionyl chloride, triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

5: 99 percent / 40percent aq. hydrofluoric acid / acetonitrile / 6 h / Ambient temperature

With pyridine; chromium(VI) oxide; n-butyllithium; thionyl chloride; hydrogen fluoride; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 115819-56-2
trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-2-methylpent-1-en-3-ol

: 115819-61-9
trans-1-<2'-methyl-2'-<4''-methyl-3''-(1'''-methylvinyl)pent-3''-enyl>cyclohexyl>prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 85 percent / butyl-lithium / tetrahydrofuran / -78 deg C, 1 h, room temperature, 1 h

3: 54 percent / thionyl chloride, triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

4: 99 percent / 40percent aq. hydrofluoric acid / acetonitrile / 6 h / Ambient temperature

With pyridine; chromium(VI) oxide; n-butyllithium; thionyl chloride; hydrogen fluoride; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;