Technology Process of C24H27N3O7
There total 5 articles about C24H27N3O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; mercury dichloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 18h;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.09.076
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 21 h / 15514.9 Torr
2: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; triethylamine; mercury dichloride;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.076
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / 18 h / Inert atmosphere; Reflux
2: sodium carbonate / water / 0 - 20 °C / Inert atmosphere
3: selenium(IV) oxide / dichloromethane / 8 h / 100 °C / Inert atmosphere; Microwave irradiation
4: palladium 10% on activated carbon; hydrogen / methanol / 21 h / 15514.9 Torr
5: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere
With
hydrogenchloride; selenium(IV) oxide; palladium 10% on activated carbon; hydrogen; sodium carbonate; triethylamine; mercury dichloride;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.076
