p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside

Base Information

Chemical Name:p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside
CAS No.:917590-92-2
Molecular Formula:C₃₂H₃₈O₆SSi
Molecular Weight:578.802
Hs Code.:

Synonyms:p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside

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Technology Process of p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside

There total 1 articles about p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 845868-93-1
1,2,3-tri-O-acetyl-5-O-t-butyldiphenylsilyl-D-arabinofuranose

: 106-45-6
para-thiocresol

: 917590-92-2
p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/ol062198j

Reference yield: 100.0%

: 917590-92-2
p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside

: 204918-55-8
p-cresyl 5-O-tert-butyldiphenylsilyl-1-thio-α-D-arabinofuranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 0.25h;
DOI:10.1021/ol062198j

Reference yield: 97.0%

: 917590-92-2
p-tolyl 5-O-t-butyldiphenylsilyl-2,3-di-O-acetyl-1-thio-α-D-arabinofuranoside

: 1268604-21-2
2,3-di-O-benzyl-α-D-arabinofuranosyl-(1->5)-3-O-benzyl-1,2-O-isopropylidene-β-D-arabinofuranose

: 1308871-84-2
2,3-di-O-acetyl-5-O-t-butyldiphenylsilyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzyl-α-D-arabinofuranosyl-(1->5)-3-O-benzyl-1,2-O-isopropylidene-β-D-arabinofuranose

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja109932t