C₁₈H₉⁽²⁾H₂F₆N₃O

Base Information

Chemical Name:C₁₈H₉⁽²⁾H₂F₆N₃O
CAS No.:1373128-27-8
Molecular Formula:C₁₈H₁₁F₆N₃O
Molecular Weight:401.279
Hs Code.:

C<sub>18</sub>H<sub>9</sub><sup>(2)</sup>H<sub>2</sub>F<sub>6</sub>N<sub>3</sub>O

Synonyms:C₁₈H₉⁽²⁾H₂F₆N₃O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₉⁽²⁾H₂F₆N₃O

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Technology Process of C₁₈H₉⁽²⁾H₂F₆N₃O

There total 4 articles about C₁₈H₉⁽²⁾H₂F₆N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1373128-34-7
2-(bromo-d2-methyl)-1-fluoro-3-(trifluoromethyl)benzene

: 1153946-38-3
2,6-difluoro-N-1H-pyrazol-4-ylbenzamide

: 1373128-27-8
C₁₈H₉⁽²⁾H₂F₆N₃O

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 72h; Inert atmosphere;

Reference yield:

: 2-fluoro-6-(trifluoromethyl)benzoyl chloride

: 1373128-27-8
C₁₈H₉⁽²⁾H₂F₆N₃O

Guidance literature:: Multi-step reaction with 4 steps

1.1: 18 h / Inert atmosphere

2.1: lithium aluminium deuteride / tetrahydrofuran / 1 h / Inert atmosphere

2.2: 0 - 20 °C / Cooling with ice

3.1: phosphorus tribromide / dichloromethane / 1.25 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C / Inert atmosphere

With lithium aluminium deuteride; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 153556-50-4
methyl 2-fluoro-6-(trifluoromethyl)benzoate

: 1373128-27-8
C₁₈H₉⁽²⁾H₂F₆N₃O

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium deuteride / tetrahydrofuran / 1 h / Inert atmosphere

1.2: 0 - 20 °C / Cooling with ice

2.1: phosphorus tribromide / dichloromethane / 1.25 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C / Inert atmosphere

With lithium aluminium deuteride; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;