4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside
CAS No.:1353638-97-7
Molecular Formula:C₂₁H₂₆N₂O₁₂
Molecular Weight:498.444
Hs Code.:

Synonyms:4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Chemical Property:

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Technology Process of 4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

There total 8 articles about 4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3459-18-5,50645-66-4
4-nitrophenyl N-acetyl-β-D-glucosaminide

: 1353638-97-7
4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: jack-bean β-hexosaminidase; water / 25 °C / pH 5.5 / aq. buffer; Enzymatic reaction

2: sodium hydride; sodium iodide / N,N-dimethyl-formamide

3: thionyl chloride / dichloromethane

4: potassium carbonate; sodium iodide / acetonitrile / 16 h / 20 °C

5: ethylenediamine / butan-1-ol / 20 h / 120 °C / Inert atmosphere

6: pyridine / 20 °C

With pyridine; thionyl chloride; jack-bean β-hexosaminidase; water; sodium hydride; potassium carbonate; ethylenediamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; butan-1-ol;
DOI:10.1080/07328303.2011.610543

Reference yield:

: 1353638-99-9
4-nitrophenylcarbamoyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 1353638-97-7
4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: hydrazine hydrate / methanol / 4 h / 20 °C

2: jack-bean β-hexosaminidase; water / 25 °C / pH 5.5 / aq. buffer; Enzymatic reaction

3: sodium hydride; sodium iodide / N,N-dimethyl-formamide

4: thionyl chloride / dichloromethane

5: potassium carbonate; sodium iodide / acetonitrile / 16 h / 20 °C

6: ethylenediamine / butan-1-ol / 20 h / 120 °C / Inert atmosphere

7: pyridine / 20 °C

With pyridine; thionyl chloride; jack-bean β-hexosaminidase; water; sodium hydride; potassium carbonate; hydrazine hydrate; ethylenediamine; sodium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; butan-1-ol;
DOI:10.1080/07328303.2011.610543

Reference yield:

: 1353638-96-6
4-nitrophenoxymethyl 2-phthalimido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 1353638-97-7
4-nitrophenoxymethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: ethylenediamine / butan-1-ol / 20 h / 120 °C / Inert atmosphere

2: pyridine / 20 °C

With pyridine; ethylenediamine; In butan-1-ol;
DOI:10.1080/07328303.2011.610543