5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Base Information

Chemical Name:5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine
CAS No.:228412-68-8
Molecular Formula:C₂₀H₂₁FN₄O₁₃
Molecular Weight:544.404
Hs Code.:

5-fluoro-N-<4-O-<methyl (β-D-glucopyranosyl)uronate>-3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Synonyms:5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Suppliers and Price of 5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

There total 4 articles about 5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 228412-67-7
5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

: 228412-68-8
5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Guidance literature:: With sodium methylate; In methanol; at -5 ℃; for 5h;

Reference yield:

: 148580-01-2
(2S,3S,4S,5R,6S)-3,4,5-Triacetoxy-6-[2-nitro-4-(4-nitro-phenoxycarbonyloxymethyl)-phenoxy]-tetrahydro-pyran-2-carboxylic acid methyl ester

: 228412-68-8
5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / NEt₃ / dimethylformamide / 18 h / Ambient temperature

2: 50 percent / pyridine / toluene; tetrahydrofuran / 4 h / Heating

3: 64 percent / NEt₃ / dimethylformamide / 18 h / Ambient temperature

4: 53 percent / NaOMe / methanol / 5 h / -5 °C

With pyridine; sodium methylate; triethylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 228412-65-5
N-<4-O--3-nitrobenzyloxycarbonyl>acetoxymethylamine

: 228412-68-8
5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / NEt₃ / dimethylformamide / 18 h / Ambient temperature

2: 53 percent / NaOMe / methanol / 5 h / -5 °C

With sodium methylate; triethylamine; In methanol; N,N-dimethyl-formamide;