C₃₄H₃₉F₃N₂O₆SSi

Base Information Edit

Chemical Name:C₃₄H₃₉F₃N₂O₆SSi
CAS No.:1374109-31-5
Molecular Formula:C₃₄H₃₉F₃N₂O₆SSi
Molecular Weight:688.84
Hs Code.:
Mol file:1374109-31-5.mol

C<sub>34</sub>H<sub>39</sub>F<sub>3</sub>N<sub>2</sub>O<sub>6</sub>SSi

Synonyms:C₃₄H₃₉F₃N₂O₆SSi

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Chemical Property of C₃₄H₃₉F₃N₂O₆SSi Edit

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Technology Process of C₃₄H₃₉F₃N₂O₆SSi

There total 7 articles about C₃₄H₃₉F₃N₂O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374108-64-1
C₁₆H₂₈O₅SSi

: 1374109-28-0
C₁₈H₁₃F₃N₂O₂

: 1374109-31-5
C₃₄H₃₉F₃N₂O₆SSi

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 18.5h; Cooling with ice;

Reference yield:

: 19315-93-6
quinoline-2,6-diol

: 1374109-31-5
C₃₄H₃₉F₃N₂O₆SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: thionyl chloride; N,N-dimethyl-formamide / 16 h / 20 °C / Cooling with ice

2.1: pyridinium p-toluenesulfonate / tetrahydrofuran / 2.5 h / 20 °C

3.1: potassium carbonate / water; 1,2-dimethoxyethane / 9 h / 80 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / Cooling with ice; Inert atmosphere

4.2: 0.17 h

5.1: trifluoroacetic acid / chloroform / 1 h / 20 °C / Cooling with ice

6.1: triethylamine / dichloromethane / 0.5 h / Cooling with ice

7.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18.5 h / 20 °C / Cooling with ice

With thionyl chloride; di-isopropyl azodicarboxylate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; triethylamine; N,N-dimethyl-formamide; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 577967-89-6
6-hydroxy-2-chloroquinoline

: 1374109-31-5
C₃₄H₃₉F₃N₂O₆SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridinium p-toluenesulfonate / tetrahydrofuran / 2.5 h / 20 °C

2.1: potassium carbonate / water; 1,2-dimethoxyethane / 9 h / 80 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / Cooling with ice; Inert atmosphere

3.2: 0.17 h

4.1: trifluoroacetic acid / chloroform / 1 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane / 0.5 h / Cooling with ice

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18.5 h / 20 °C / Cooling with ice

With di-isopropyl azodicarboxylate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; mineral oil;