C₁₂H₁₁BrO₂

Base Information

Chemical Name:C₁₂H₁₁BrO₂
CAS No.:1311148-17-0
Molecular Formula:C₁₂H₁₁BrO₂
Molecular Weight:267.122
Hs Code.:

C<sub>12</sub>H<sub>11</sub>BrO<sub>2</sub>

Synonyms:C₁₂H₁₁BrO₂

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Chemical Property of C₁₂H₁₁BrO₂

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Technology Process of C₁₂H₁₁BrO₂

There total 3 articles about C₁₂H₁₁BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1311148-16-9
C₁₅H₁₅BrO₃

: 1311148-17-0
C₁₂H₁₁BrO₂

Guidance literature:: C₁₅H₁₅BrO₃; With diisobutylaluminium hydride; In toluene; at -78 ℃; for 0.25h; Inert atmosphere;

With Rochelle's salt; In water; toluene; at -78 ℃; Inert atmosphere;
DOI:10.1021/ol201390r

Reference yield:

: 1311148-31-8,246530-08-5
(E)-3-(2-bromophenyl)-2-methylacrylaldehyde

: 1311148-17-0
C₁₂H₁₁BrO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 80 °C

2.1: diisobutylaluminium hydride / toluene / 0.25 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

With diisobutylaluminium hydride; In toluene; 1.1: Wittig reaction;
DOI:10.1021/ol201390r

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1311148-17-0
C₁₂H₁₁BrO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / methanol; water / 72 h / 20 °C

2.1: toluene / 80 °C

3.1: diisobutylaluminium hydride / toluene / 0.25 h / -78 °C / Inert atmosphere

3.2: -78 °C / Inert atmosphere

With diisobutylaluminium hydride; sodium hydroxide; In methanol; water; toluene; 2.1: Wittig reaction;
DOI:10.1021/ol201390r