C₂₄H₃₆O₅Si

Base Information

Chemical Name:C₂₄H₃₆O₅Si
CAS No.:1388152-95-1
Molecular Formula:C₂₄H₃₆O₅Si
Molecular Weight:432.632
Hs Code.:

C<sub>24</sub>H<sub>36</sub>O<sub>5</sub>Si

Synonyms:C₂₄H₃₆O₅Si

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Chemical Property of C₂₄H₃₆O₅Si

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Technology Process of C₂₄H₃₆O₅Si

There total 18 articles about C₂₄H₃₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1388153-30-7
C₂₄H₃₇ClO₅Si

: 1388152-95-1
C₂₄H₃₆O₅Si

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -40 ℃; for 0.75h; Inert atmosphere;
DOI:10.1021/ja305864z

Reference yield:

: C₂₆H₄₀O₆Si

: 1388152-95-1
C₂₄H₃₆O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

2.2: -20 °C / Molecular sieve

3.1: N-chloro-succinimide; triphenylphosphine; methyloxirane / dichloromethane / 0.75 h / 0 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -40 °C / Inert atmosphere

With titanium(IV) isopropylate; N-chloro-succinimide; (-)-diethyl tartrate; diisobutylaluminium hydride; triphenylphosphine; methyloxirane; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-25-0
C₂₇H₄₈O₅Si₂

: 1388152-95-1
C₂₄H₃₆O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

2.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 2 h / -78 - 0 °C

4.1: tetrahydrofuran / 0.5 h / 20 °C

5.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

6.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1.5 h / 20 °C

6.2: 1 h / 20 °C

7.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

8.2: -20 °C / Molecular sieve

9.1: N-chloro-succinimide; triphenylphosphine; methyloxirane / dichloromethane / 0.75 h / 0 °C

10.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -40 °C / Inert atmosphere

With titanium(IV) isopropylate; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; (-)-diethyl tartrate; camphor-10-sulfonic acid; potassium tert-butylate; dihydrogen peroxide; sulfur trioxide pyridine complex; diisobutylaluminium hydride; triethylamine; triphenylphosphine; methyloxirane; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; 8.1: Sharpless epoxidation / 8.2: Sharpless epoxidation;
DOI:10.1021/ja305864z