2-iodobenzoyl fluoride

Base Information

• Chemical Name: 2-iodobenzoyl fluoride
• CAS No.: 1064679-44-2
• Molecular Formula: C₇H₄FIO
• Molecular Weight: 250.011

Synonyms:2-iodobenzoyl fluoride

Chemical Property of 2-iodobenzoyl fluoride

Chemical Property:

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Technology Process of 2-iodobenzoyl fluoride

There total 3 articles about 2-iodobenzoyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-Iodobenzoic acid (88-67-5) → 2-iodobenzoyl fluoride (1064679-44-2)

Guidance literature:

With pyridine; thionyl fluoride; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1039/d1sc05316g

Reference yield: 13.0%

Togni's reagent II (887144-94-7) → 2-iodobenzoyl fluoride (1064679-44-2)

Guidance literature:

With 4-tert-butylanisole; In d₇-N,N-dimethylformamide; at 60 ℃; for 1.5h;

DOI:10.1021/jo8014825

Reference yield:

Br(1-)*C25H19IO2P(1+) → 2-iodobenzoyl fluoride (1064679-44-2)

Guidance literature:

With triethylamine tris(hydrogen fluoride); at 20 ℃; for 2h;

DOI:10.1021/acs.orglett.9b00197

upstream raw materials:

Togni's reagent II

2-Iodobenzoic acid

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