2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime

Base Information

Chemical Name:2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime
CAS No.:152877-34-4
Molecular Formula:C₂₀H₁₉F₃N₂O₄S
Molecular Weight:440.443
Hs Code.:

Synonyms:2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime

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Chemical Property of 2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime

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Technology Process of 2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime

There total 1 articles about 2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 98-59-9
p-toluenesulfonyl chloride

: 2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone oxime

: 152877-34-4
2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.3987/COM-92-S(T)93

Reference yield: 100.0%

: 152877-34-4
2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime

: 152042-96-1
3-<(4,4-dimethyl-2-oxazolyl)phenyl>-3-trifluoromethyldiaziridine

Guidance literature:: With ammonia; In dichloromethane; for 6h; Ambient temperature;
DOI:10.3987/COM-92-S(T)93

Reference yield:

: 152877-34-4
2,2,2-trifluoro-1-<4-(4,4-dimethyl-2-oxazolyl)phenyl>-1-ethanone O-(p-tolylsulfonyl)oxime

: 152042-97-2
3-<(4,4-dimethyl-2-oxazolyl)phenyl>-3-trifluoromethyl-3H-diazirine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / liq. ammonia / CH₂Cl₂ / 6 h / Ambient temperature

2: 87 percent / tert-butyl hypochlorite, triethylamine / 2-methyl-propan-2-ol; ethanol / 0.5 h / 0 °C

With tert-butylhypochlorite; ammonia; triethylamine; In ethanol; dichloromethane; tert-butyl alcohol;
DOI:10.3987/COM-92-S(T)93