Technology Process of C53H56O2
There total 7 articles about C53H56O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
Heating;
DOI:10.1246/cl.2006.168
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 75 percent / triethylamine / Pd(PPh3)4; CuI / tetrahydrofuran / 55 °C
2: 90 percent / MeI / 125 °C / sealed tube
3: 52 percent / CH3(C8H17)3NCl; PPh3; KOH / Pd(PPh3)4; CuI / benzene; H2O / 85 °C
4: 92 percent / K2CO3 / Pd(PPh3)4 / tetrahydrofuran / Heating
With
potassium hydroxide; potassium carbonate; triethylamine; triphenylphosphine; methyl iodide;
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; water; benzene;
1: Sonogashira coupling / 3: double Sonogashira coupling / 4: Suzuki-Miyaura coupling;
DOI:10.1246/cl.2006.168
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 52 percent / CH3(C8H17)3NCl; PPh3; KOH / Pd(PPh3)4; CuI / benzene; H2O / 85 °C
2: 92 percent / K2CO3 / Pd(PPh3)4 / tetrahydrofuran / Heating
With
potassium hydroxide; potassium carbonate; triphenylphosphine;
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; water; benzene;
1: double Sonogashira coupling / 2: Suzuki-Miyaura coupling;
DOI:10.1246/cl.2006.168
