4-acetamido-1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2-pyrimidinone

Base Information

Chemical Name:4-acetamido-1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2-pyrimidinone
CAS No.:107712-10-7
Molecular Formula:C₃₃H₂₆N₆O₁₅
Molecular Weight:746.601
Hs Code.:

Synonyms:4-acetamido-1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2-pyrimidinone

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Chemical Property of 4-acetamido-1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2-pyrimidinone

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Technology Process of 4-acetamido-1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2-pyrimidinone

There total 2 articles about 4-acetamido-1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2-pyrimidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 107712-26-5
bis-O-(trimethylsilyl)-N-acetylcytosine

: 107796-01-0
2-deoxy-1,3,4,6-tetrakis-O-(4-nitrobenzoyl)-α-D-ribo-hexopyranose

: 107712-10-7
4-acetamido-1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2-pyrimidinone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 25 ℃; for 240h;
DOI:10.1021/jm00389a015

Reference yield:

: 14631-20-0
4-N-Acetylcytosine

: 107712-10-7
4-acetamido-1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2-pyrimidinone

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium sulfate / 8 h / 135 °C

2: 82 percent / trimethylsilyl trifluoromethanesulfonate (TMS-triflate) / acetonitrile / 240 h / 25 °C

With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; In acetonitrile;
DOI:10.1021/jm00389a015