C₆₁H₉₃NO₈

Base Information

Chemical Name:C₆₁H₉₃NO₈
CAS No.:1282034-27-8
Molecular Formula:C₆₁H₉₃NO₈
Molecular Weight:968.411
Hs Code.:

C<sub>61</sub>H<sub>93</sub>NO<sub>8</sub>

Synonyms:C₆₁H₉₃NO₈

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Chemical Property of C₆₁H₉₃NO₈

Chemical Property:

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Technology Process of C₆₁H₉₃NO₈

There total 15 articles about C₆₁H₉₃NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1282034-42-7
C₈₀H₁₀₇NO₈

: 1282034-27-8
C₆₁H₉₃NO₈

Guidance literature:: With Pd(OH)2 (10% on C); hydrogen; In ethyl acetate; at 20 ℃; for 24h;
DOI:10.1002/anie.201006035

Reference yield:

: C₃₀H₅₀O₂

: 1282034-27-8
C₆₁H₉₃NO₈

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine; dmap / 18 h / 20 °C / Inert atmosphere

2: Pd(OH)2 (10% on C); hydrogen / ethyl acetate / 5 h / 20 °C

3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 6 h / 20 °C

4: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 0 - 20 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

6: pyridine / 20 - 50 °C / Inert atmosphere

7: pyridine; dmap / 50 °C / Inert atmosphere

8: Pd(OH)2 (10% on C); hydrogen / ethyl acetate / 24 h / 20 °C

With pyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Pd(OH)2 (10% on C); hydrogen; sodium hydrogencarbonate; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; pyridine; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1002/anie.201006035

Reference yield:

: 1282034-25-6
C₃₇H₅₄O₃

: 1282034-27-8
C₆₁H₉₃NO₈

Guidance literature:: Multi-step reaction with 7 steps

1: Pd(OH)2 (10% on C); hydrogen / ethyl acetate / 5 h / 20 °C

2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 6 h / 20 °C

3: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 0 - 20 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

5: pyridine / 20 - 50 °C / Inert atmosphere

6: pyridine; dmap / 50 °C / Inert atmosphere

7: Pd(OH)2 (10% on C); hydrogen / ethyl acetate / 24 h / 20 °C

With pyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Pd(OH)2 (10% on C); hydrogen; sodium hydrogencarbonate; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; pyridine; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1002/anie.201006035