ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate

Base Information

Chemical Name:ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate
CAS No.:1381931-68-5
Molecular Formula:C₂₄H₂₁BrO₇
Molecular Weight:501.331
Hs Code.:

Synonyms:ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate

Suppliers and Price of ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate

There total 6 articles about ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 948049-20-5
C₁₀H₁₁BrO₃

: 1381931-76-5
ethyl 6-formyl-8-methyl-2-oxo-2H-chromene-3-carboxylate

: 1381931-68-5
ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate

Guidance literature:: With hydrogenchloride; In acetonitrile; at 5 ℃; for 18h;
DOI:10.1016/j.bmcl.2012.04.100

Reference yield:

: 1381931-79-8
(Z)-3-(4-bromophenyl)but-2-en-1-ol

: 1381931-68-5
ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: oxygen; methylene blue / acetonitrile / 6 h / -10 - 0 °C / Irradiation

2: hydrogenchloride / acetonitrile / 18 h / 5 °C

With hydrogenchloride; oxygen; methylene blue; In acetonitrile;
DOI:10.1016/j.bmcl.2012.04.100

Reference yield:

: 3328-73-2
4-hydroxy-5-methylisophthalaldehyde

: 1381931-68-5
ethyl 6-(6-(1-(4-bromophenyl)vinyl)-1,2,4-trioxan-3-yl)-8-methyl-2-oxo-2H-chromene carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 0.5 h / Reflux

2: hydrogenchloride / acetonitrile / 18 h / 5 °C

With piperidine; hydrogenchloride; In ethanol; acetonitrile;
DOI:10.1016/j.bmcl.2012.04.100