C₂₂H₃₀O₃

Base Information

Chemical Name:C₂₂H₃₀O₃
CAS No.:1577210-22-0
Molecular Formula:C₂₂H₃₀O₃
Molecular Weight:342.478
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>3</sub>

Synonyms:C₂₂H₃₀O₃

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Chemical Property of C₂₂H₃₀O₃

Chemical Property:

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Technology Process of C₂₂H₃₀O₃

There total 12 articles about C₂₂H₃₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1577210-18-4
C₂₂H₃₂O₃

: 1577210-22-0
C₂₂H₃₀O₃

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ja413106t

Reference yield:

: 1577209-95-0
C₂₆H₃₈O₄Si

: 1577210-22-0
C₂₂H₃₀O₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: selenium(IV) oxide; tert.-butylhydroperoxide / dichloromethane; water / 16 h / 20 °C / Inert atmosphere

2.1: [Rh(nbd)(diphos-4)]BF₄; hydrogen / tetrahydrofuran / 2 h / 20 °C / 31029.7 Torr

3.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6.33 h / 0 - 20 °C / Inert atmosphere

5.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

6.1: trimethylphosphane; titanium(IV) isopropylate / tetrahydrofuran / 3 h / 70 °C / Inert atmosphere

7.1: cerium(III) chloride heptahydrate / tetrahydrofuran / 0.25 h / 20 °C / Schlenk technique; Inert atmosphere

7.2: 0.25 h / 0 °C / Schlenk technique; Inert atmosphere

8.1: titanium tetrachloride / dichloromethane; toluene / 0.25 h / 0 °C / Inert atmosphere

8.2: 0.5 h / -78 °C / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 36 h / 65 °C / Inert atmosphere

10.1: hydrogen; palladium 10% on activated carbon / methanol / 5 h

11.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; selenium(IV) oxide; cerium(III) chloride heptahydrate; palladium 10% on activated carbon; [Rh(nbd)(diphos-4)]BF₄; tetrabutyl ammonium fluoride; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; trimethylphosphane; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1021/ja413106t

Reference yield:

: 1577209-97-2
C₂₆H₃₈O₅Si

: 1577210-22-0
C₂₂H₃₀O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: [Rh(nbd)(diphos-4)]BF₄; hydrogen / tetrahydrofuran / 2 h / 20 °C / 31029.7 Torr

2.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6.33 h / 0 - 20 °C / Inert atmosphere

4.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

5.1: trimethylphosphane; titanium(IV) isopropylate / tetrahydrofuran / 3 h / 70 °C / Inert atmosphere

6.1: cerium(III) chloride heptahydrate / tetrahydrofuran / 0.25 h / 20 °C / Schlenk technique; Inert atmosphere

6.2: 0.25 h / 0 °C / Schlenk technique; Inert atmosphere

7.1: titanium tetrachloride / dichloromethane; toluene / 0.25 h / 0 °C / Inert atmosphere

7.2: 0.5 h / -78 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 36 h / 65 °C / Inert atmosphere

9.1: hydrogen; palladium 10% on activated carbon / methanol / 5 h

10.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; titanium(IV) isopropylate; cerium(III) chloride heptahydrate; palladium 10% on activated carbon; [Rh(nbd)(diphos-4)]BF₄; tetrabutyl ammonium fluoride; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; trimethylphosphane; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja413106t