(Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide

Base Information

Chemical Name:(Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide
CAS No.:26926-78-3
Molecular Formula:C₂₅H₂₆P*I
Molecular Weight:484.36
Hs Code.:

Synonyms:(Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide

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Chemical Property of (Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide

Chemical Property:

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Technology Process of (Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide

There total 5 articles about (Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 26926-75-0
(Z)-6-iodo-3-methylhexa-1,3-diene

: 603-35-0
triphenylphosphine

: 26926-78-3
(Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃; for 4h;
DOI:10.1039/P19850000399

Reference yield:

: 4378-02-3
2-cyclopropylbut-3-yn-2-ol

: 26926-78-3
(Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 48percent HBr / 0.25 h

2: 86 percent / H₂, quinoline / Pd/BaSO₄ / methanol / 39 h / 760 Torr

3: NaI / acetone / 8 h / Heating

4: 88 percent / dimethylformamide / 4 h / 100 °C

With quinoline; hydrogen bromide; hydrogen; sodium iodide; Pd-BaSO₄; In methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1039/P19850000399

Reference yield:

: 96890-20-9
(Z)-6-bromo-3-methylhex-3-en-1-yne

: 26926-78-3
(Z)-4-methylhexa-3,5-dienyltriphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / H₂, quinoline / Pd/BaSO₄ / methanol / 39 h / 760 Torr

2: NaI / acetone / 8 h / Heating

3: 88 percent / dimethylformamide / 4 h / 100 °C

With quinoline; hydrogen; sodium iodide; Pd-BaSO₄; In methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1039/P19850000399