N¹-methoxycarbonyl-N²-benzyl-N²-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine

Base Information

• Chemical Name: N¹-methoxycarbonyl-N²-benzyl-N²-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine
• CAS No.: 132611-17-7
• Molecular Formula: C₂₀H₁₉N₅O₅
• Molecular Weight: 409.401

Synonyms:N¹-methoxycarbonyl-N²-benzyl-N²-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine

Chemical Property of N¹-methoxycarbonyl-N²-benzyl-N²-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N¹-methoxycarbonyl-N²-benzyl-N²-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine

There total 1 articles about N¹-methoxycarbonyl-N²-benzyl-N²-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N1-benzyl-N2-methoxycarbonylhydrazine (69353-11-3) + 5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acid (69195-96-6) → N1-methoxycarbonyl-N2-benzyl-N2-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine (132611-17-7)

Guidance literature:

With 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1) THF, reflux, ca. 1.5 h 2) r.t., 4-5 h;

DOI:10.1055/s-1990-27103

Reference yield: 73.0%

N1-methoxycarbonyl-N2-benzyl-N2-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine (132611-17-7) → N1-methoxycarbonyl-N2-benzyl-N2-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine (132611-18-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 1.5h; under 2327.2 Torr;

DOI:10.1055/s-1990-27103

Reference yield: 67.0%

N1-methoxycarbonyl-N2-benzyl-N2-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine (132611-17-7) → 3,7-dibenzyl-3,4,6,7-tetrahydroimidazo<4,5-e><1,2,4>triazepine-5,8-dione (132611-23-5)

Guidance literature:

With potassium hydroxide; sodium tetrahydroborate; palladium on activated charcoal; In ethanol; 1) r.t., 1 h 2) reflux, 2 h;

DOI:10.1055/s-1990-27103

upstream raw materials:

N¹-benzyl-N²-methoxycarbonylhydrazine

5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acid

Downstream raw materials:

3,7-dibenzyl-3,4,6,7-tetrahydroimidazo<4,5-e><1,2,4>triazepine-5,8-dione

N¹-methoxycarbonyl-N²-benzyl-N²-(5-amino-1-benzyl-4-imidazolylcarbonyl)hydrazine

7-benzyl-3,4,6,7-tetrahydroimidazo<4,5-e><1,2,4>triazepine-5,8-dione

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 132611-17-7 N¹-methoxycarbonyl-N²-benzyl-N²-(1-benzyl-5-nitro-4-imidazolylcarbonyl)hydrazine

Send

Send

Metric Ton KG G Pound L ML

Send

Send