1-bromo-2,4-diiodobenzene

Base Information

• Chemical Name: 1-bromo-2,4-diiodobenzene
• CAS No.: 126063-04-5
• Molecular Formula: C₆H₃BrI₂
• Molecular Weight: 408.803
• Mol file: 126063-04-5.mol

Synonyms:1-bromo-2,4-diiodobenzene

Chemical Property of 1-bromo-2,4-diiodobenzene

Chemical Property:

• Boiling Point: 337.3±22.0 °C(Predicted)
• Density: 2.729±0.06 g/cm3(Predicted)

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-bromo-2,4-diiodobenzene

There total 1 articles about 1-bromo-2,4-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

bromobenzene (108-86-1,52753-63-6) → 4-bromo-1,2,-diiodobenzene (21521-54-0) + 1-bromo-2,4-diiodobenzene (126063-04-5) + 1-bromo-2,4,5-triiodothiophene (126063-05-6)

Guidance literature:

With iodine; fluorine; In chloroform; trichlorofluoromethane; at 25 ℃; for 6h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/jo00298a032

Reference yield: 76.8%

4-dibenzofurylboronic acid (100124-06-9) + 1-bromo-2,4-diiodobenzene (126063-04-5) → C18H10BrIO

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; In 1,2-dimethoxyethane; water; at 60 ℃; for 10h; Inert atmosphere;

upstream raw materials:

bromobenzene

Refernces