10,13-dimethylpentaheliceno[7,8-c]furan-3,5-dione

Base Information

Chemical Name:10,13-dimethylpentaheliceno[7,8-c]furan-3,5-dione
CAS No.:7499-48-1
Molecular Formula:C₂₆H₁₆O₃
Molecular Weight:376.411
Hs Code.:

Synonyms:9,12-dimethyl-dibenzo[c,g]phenanthrene-3,4-dicarboxylic acid-anhydride

Suppliers and Price of 10,13-dimethylpentaheliceno[7,8-c]furan-3,5-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 10,13-dimethylpentaheliceno[7,8-c]furan-3,5-dione

Chemical Property:

Vapor Pressure:8.44E-18mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10,13-dimethylpentaheliceno[7,8-c]furan-3,5-dione

There total 4 articles about 10,13-dimethylpentaheliceno[7,8-c]furan-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7499-49-2
9,12-dimethyl-1,2,5,6-tetrahydro-dibenzo[c,g]phenanthrene-3,4-dicarboxylic acid-anhydride

: 7499-48-1
9,12-dimethyl-dibenzo[c,g]phenanthrene-3,4-dicarboxylic acid-anhydride

Guidance literature:: With palladium on activated charcoal; at 350 ℃;
DOI:10.1021/ja01864a014

Reference yield:

: 22009-37-6
7-methyl-3,4-dihydro-2H-naphthalen-1-one

: 7499-48-1
9,12-dimethyl-dibenzo[c,g]phenanthrene-3,4-dicarboxylic acid-anhydride

Guidance literature:: Multi-step reaction with 4 steps

1: amalgamated aluminium; ethanol; benzene / Erhitzen des Reaktionsprodukts in Eisessig

2: xylene

3: lead (IV)-acetate; acetic acid anhydride; acetic acid

4: palladium/charcoal / 350 °C

With lead(IV) acetate; palladium on activated charcoal; ethanol; aluminium amalgam; acetic anhydride; acetic acid; xylene; benzene;
DOI:10.1021/ja01864a014

Reference yield:

: 7499-37-8
7,7'-Dimethyl-3,4,3',4'-tetrahydro-[1,1']binaphthyl

: 7499-48-1
9,12-dimethyl-dibenzo[c,g]phenanthrene-3,4-dicarboxylic acid-anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: xylene

2: lead (IV)-acetate; acetic acid anhydride; acetic acid

3: palladium/charcoal / 350 °C

With lead(IV) acetate; palladium on activated charcoal; acetic anhydride; acetic acid; xylene;
DOI:10.1021/ja01864a014