3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

Base Information

Chemical Name:3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose
CAS No.:115996-14-0
Molecular Formula:C₁₆H₂₃NO₇S
Molecular Weight:373.427
Hs Code.:

Synonyms:3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

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Chemical Property of 3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

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Technology Process of 3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

There total 4 articles about 3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22169-72-8
3-azido-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

: 115996-14-0
3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 10h; under 760 Torr; Ambient temperature;

Reference yield:

: 22169-71-7
(R)-1-((3aR,5S,6S,6aR)-6-azido-2,2-dimethyltetrahydrofuro-[2,3-d][1,3]dioxol-5-yl)ethane-1,2-diol

: 115996-14-0
3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 0.90 g / pyridine / CHCl₃ / 16 h / 20 °C

2: 0.64 g / H₂ / Raney nickel / ethanol / 1 h / 760 Torr

With pyridine; hydrogen; nickel; In ethanol; chloroform;
DOI:10.1021/jm00152a012

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 115996-14-0
3-amino-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 0.90 g / pyridine / CHCl₃ / 16 h / 20 °C

2: 0.64 g / H₂ / Raney nickel / ethanol / 1 h / 760 Torr

With pyridine; hydrogen; nickel; In ethanol; chloroform;
DOI:10.1021/jm00152a012