N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester

Base Information

Chemical Name:N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester
CAS No.:128950-25-4
Molecular Formula:C₃₃H₃₉NO₆
Molecular Weight:545.676
Hs Code.:

Synonyms:N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester

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Chemical Property of N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester

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Technology Process of N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester

There total 3 articles about N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 67326-20-9
3-carbethoxybenzoyl chloride

: 128950-23-2
ethyl 2-<(6-phenylhexyl)oxy>-5-aminobenzenepropanoate

: 128950-25-4
N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester

Guidance literature:: With pyridine; at 25 ℃; for 2h;
DOI:10.1021/jm00172a019

Reference yield:

: 20921-04-4
ethyl 3-(2-hydroxyphenyl)propanoate

: 128950-25-4
N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 28 percent / con. HNO₃, acetic acid / 0.5 h / 0 °C

2: H₂ / 10percent Pd/C / ethyl acetate / 1 h / 1551.4 Torr

3: 41 percent / pyridine / 2 h / 25 °C

With pyridine; hydrogen; nitric acid; acetic acid; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jm00172a019

Reference yield:

: 20921-11-3
ethyl 3-(2-hydroxy-5-nitrophenyl)propanoate

: 128950-25-4
N-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-phenyl]-isophthalamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethyl acetate / 1 h / 1551.4 Torr

2: 41 percent / pyridine / 2 h / 25 °C

With pyridine; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jm00172a019