mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

Base Information

Chemical Name:mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate
CAS No.:945916-03-0
Molecular Formula:C₃₁H₃₂O₆
Molecular Weight:500.591
Hs Code.:

Synonyms:mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

Suppliers and Price of mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

There total 2 articles about mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 945916-13-2
(1Z,4E)-4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoic acid

: 527-60-6
Mesitol

: 945916-03-0
mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃;
DOI:10.1002/ejoc.200700156

Reference yield:

: ethyl (1Z,4E)-4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

: 945916-03-0
mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol; H₂O / 9 h / 55 °C

2: 46 percent / DMAP; DCC / CH₂Cl₂ / 0 °C

With dmap; potassium hydroxide; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water;
DOI:10.1002/ejoc.200700156

Reference yield: 99.0%

: 945916-03-0
mesityl 4-methyl-3-oxo-5-phenyl-2-(2,4,6-trimethoxybenzylidene)pent-4-enoate

: mesityl 3-methyl-2-oxo-4-phenyl-5-(2,4,6-trimethoxyphenyl)cyclopent-3-ene-1-carboxylate

Guidance literature:: With silver hexafluoroantimonate; vanadium(IV)(salen)Cl₂; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1002/ejoc.200700156