Technology Process of 8-(2,3-dimethoxyphenyl)-6-methoxy-2-phenethyl-1,2,3,4-tetrahydroisoquinolin-7-ol
There total 4 articles about 8-(2,3-dimethoxyphenyl)-6-methoxy-2-phenethyl-1,2,3,4-tetrahydroisoquinolin-7-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; sodium carbonate; triphenylphosphine;
In
water; isopropyl alcohol;
at 120 ℃;
for 0.166667h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: isopropyl alcohol / 15 h / Reflux
1.2: 0.17 h / Inert atmosphere
2.1: lead(IV) tetraacetate; acetic acid / 20 °C
2.2: 20 °C
3.1: triphenylphosphine; sodium carbonate; palladium diacetate / isopropyl alcohol; water / 0.17 h / 120 °C / Microwave irradiation
With
lead(IV) tetraacetate; palladium diacetate; sodium carbonate; acetic acid; triphenylphosphine;
In
water; isopropyl alcohol;
3.1: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: isopropyl alcohol / 15 h / Reflux
1.2: 0.17 h / Inert atmosphere
2.1: lead(IV) tetraacetate; acetic acid / 20 °C
2.2: 20 °C
3.1: triphenylphosphine; sodium carbonate; palladium diacetate / isopropyl alcohol; water / 0.17 h / 120 °C / Microwave irradiation
With
lead(IV) tetraacetate; palladium diacetate; sodium carbonate; acetic acid; triphenylphosphine;
In
water; isopropyl alcohol;
3.1: |Suzuki Coupling;
