bis(monomethyl phthalate)diethyltin

Base Information

Chemical Name:bis(monomethyl phthalate)diethyltin
CAS No.:915772-91-7
Molecular Formula:C₂₂H₂₄O₈Sn
Molecular Weight:535.138
Hs Code.:

Synonyms:bis(monomethyl phthalate)diethyltin

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Chemical Property of bis(monomethyl phthalate)diethyltin

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Technology Process of bis(monomethyl phthalate)diethyltin

There total 1 articles about bis(monomethyl phthalate)diethyltin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 4376-18-5
Monomethyl phthalate

: 866-55-7
dichlorodiethylstannane

: 915772-91-7
bis(monomethyl phthalate)diethyltin

Guidance literature:: With triethylamine; In methanol; byproducts: triethylamine chloride; (N2); addn. of Et3N (1 equiv.) to hot methanolic soln. of monomethyl phthalate (1 equiv.); reflux for 0.5 h; addn. dropwise of soln. of SnCl2Et2(0.5 equiv.) in MeOH with constant stirring; reflux for 8-10 h; centrifugating; evapn. of solvent under vac.; recrystn. from CHCl3 and petroleum ether (40-60°C); elem. anal.;
DOI:10.1016/j.saa.2005.12.031