bis(monomethyl phthalate)diethyltin

Base Information

• Chemical Name: bis(monomethyl phthalate)diethyltin
• CAS No.: 915772-91-7
• Molecular Formula: C₂₂H₂₄O₈Sn
• Molecular Weight: 535.138
• Mol file: 915772-91-7.mol

Synonyms:bis(monomethyl phthalate)diethyltin

Chemical Property of bis(monomethyl phthalate)diethyltin

Chemical Property:

Purity/Quality:

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Technology Process of bis(monomethyl phthalate)diethyltin

There total 1 articles about bis(monomethyl phthalate)diethyltin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

Monomethyl phthalate (4376-18-5) + dichlorodiethylstannane (866-55-7) → bis(monomethyl phthalate)diethyltin (915772-91-7)

Guidance literature:

With triethylamine; In methanol; byproducts: triethylamine chloride; (N2); addn. of Et3N (1 equiv.) to hot methanolic soln. of monomethyl phthalate (1 equiv.); reflux for 0.5 h; addn. dropwise of soln. of SnCl2Et2(0.5 equiv.) in MeOH with constant stirring; reflux for 8-10 h; centrifugating; evapn. of solvent under vac.; recrystn. from CHCl3 and petroleum ether (40-60°C); elem. anal.;

DOI:10.1016/j.saa.2005.12.031

upstream raw materials:

Monomethyl phthalate

dichlorodiethylstannane