12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole

Base Information

Chemical Name:12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole
CAS No.:934506-88-4
Molecular Formula:C₃₇H₃₁N₃O₄
Molecular Weight:581.671
Hs Code.:

Synonyms:12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole

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Chemical Property of 12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole

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Technology Process of 12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole

There total 3 articles about 12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934506-81-7
12-benzyl-5-cyano-11,12-dihydroindolo[2,3-a]carbazole

: 934506-88-4
12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / NaBH₄; CoCl₂*6H₂O / methanol; tetrahydrofuran / 1 h / 20 °C

2: MS₄ Angstroem / tetrahydrofuran / 2 h / Heating

3: NaBH₄ / methanol / 1 h / 20 °C

4: 50 percent / Cu(OAc)2; air / Pd(OAc)2 / dimethylsulfoxide / 12 h / 110 °C / 760 Torr

With sodium tetrahydroborate; copper diacetate; air; MS₄ Angstroem; cobalt(II) chloride; palladium diacetate; In tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1021/jo062184r

Reference yield:

: 934506-84-0
12-benzyl-5-(aminomethyl)-11,12-dihydroindolo[2,3-a]carbazole

: 934506-88-4
12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: MS₄ Angstroem / tetrahydrofuran / 2 h / Heating

2: NaBH₄ / methanol / 1 h / 20 °C

3: 50 percent / Cu(OAc)2; air / Pd(OAc)2 / dimethylsulfoxide / 12 h / 110 °C / 760 Torr

With sodium tetrahydroborate; copper diacetate; air; MS₄ Angstroem; palladium diacetate; In tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1021/jo062184r

Reference yield:

: (12-benzyl-11,12-dihydro-11,12-diaza-indeno[2,1-a]fluoren-5-ylmethyl)-(2,4,6-trimethoxy-benzylidene)-amine

: 934506-88-4
12-benzyl-6-(2,4,6-trimethoxybenzyl)indolo[2,3-a]pyrrolo[3,4-c]carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 1 h / 20 °C

2: 50 percent / Cu(OAc)2; air / Pd(OAc)2 / dimethylsulfoxide / 12 h / 110 °C / 760 Torr

With sodium tetrahydroborate; copper diacetate; air; palladium diacetate; In methanol; dimethyl sulfoxide;
DOI:10.1021/jo062184r