C₁₇H₂₈O₃S

Base Information

• Chemical Name: C₁₇H₂₈O₃S
• CAS No.: 884843-07-6
• Molecular Formula: C₁₇H₂₈O₃S
• Molecular Weight: 312.474
• Mol file: 884843-07-6.mol

Synonyms:C₁₇H₂₈O₃S

Chemical Property of C₁₇H₂₈O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₇H₂₈O₃S

There total 1 articles about C₁₇H₂₈O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-bromo-10-decanol (53463-68-6) + methylphenylsulfonate (3112-85-4) → C17H28O3S (884843-07-6)

Guidance literature:

methylphenylsulfonate; With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -78 ℃; for 0.5h;

1-bromo-10-decanol; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -78 - 20 ℃; for 8h; Further stages.;

DOI:10.1271/bbb.69.1620

Reference yield:

C17H28O3S (884843-07-6) → C39H68O2S (884843-10-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 99 percent / oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -78 - 20 °C

2.1: 91 percent / potassium hexamethyldisilazide / tetrahydrofuran; toluene; hexamethylphosphoric acid triamide / -78 - 20 °C

3.1: butyllithium / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide / 0.02 h / -78 °C

3.2: 62 percent / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - 20 °C

With n-butyllithium; oxalyl dichloride; potassium hexamethylsilazane; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; toluene; 1.1: Swern oxidation / 2.1: Wittig olefination;

DOI:10.1271/bbb.69.1620

Reference yield:

C17H28O3S (884843-07-6) → C23H38O2S (884843-09-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -78 - 20 °C

2: 91 percent / potassium hexamethyldisilazide / tetrahydrofuran; toluene; hexamethylphosphoric acid triamide / -78 - 20 °C

With oxalyl dichloride; potassium hexamethylsilazane; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene; 1: Swern oxidation / 2: Wittig olefination;

DOI:10.1271/bbb.69.1620

upstream raw materials:

1-bromo-10-decanol

methylphenylsulfonate

Downstream raw materials:

C₂₃H₃₈O₂S

C₃₉H₆₈O₂S