{2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane

Base Information

• Chemical Name: {2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane
• CAS No.: 929007-22-7
• Molecular Formula: C₄₂H₄₀O₇P₂
• Molecular Weight: 718.723

Synonyms:{2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane

Chemical Property of {2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane

Chemical Property:

Purity/Quality:

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Technology Process of {2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane

There total 1 articles about {2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[{2'-[bis-(3-methoxy-phenyl)-phosphanyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-λ5-phosphanylidene]-acetic acid ethyl ester + 2-phenylpent-1-en-1-one (57768-76-0) → 4-phenylhepta-2,3-dienoic acid ethyl ester + 4-phenylhepta-2,3-dienoic acid ethyl ester + {2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane (929007-22-7)

Guidance literature:

With sodium bromide; In tetrahydrofuran; toluene; at -65 ℃; for 72h; Title compound not separated from byproducts;

DOI:10.1021/ja068642v

Reference yield: 85.2%

{2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane (929007-22-7) → 2,2'-bis-[bis-(3-methoxy-phenyl)-phosphanyl]-6,6'-dimethoxy-biphenyl

Guidance literature:

With trichlorosilane; N,N-dimethyl-aniline; In toluene; Heating;

DOI:10.1021/ja068642v

Reference yield:

{2'-[bis-(3-methoxy-phenyl)-phosphinoyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-phosphane (929007-22-7) → [{2'-[bis-(3-methoxy-phenyl)-phosphanyl]-6,6'-dimethoxy-biphenyl-2-yl}-bis-(3-methoxy-phenyl)-λ5-phosphanylidene]-acetic acid ethyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: 85.2 percent / N,N-dimethylaniline; trichlorosilane / toluene / Heating

2: tetra(p-chlorophenyl)porphyrin iron chloride / toluene / 20 °C

With trichlorosilane; N,N-dimethyl-aniline; [5,10,15,20-tetrakis(4-chlorophenyl)porphyrinato]iron(III) chloride; In toluene;

DOI:10.1021/ja068642v

upstream raw materials:

2-phenylpent-1-en-1-one

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