but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide

Base Information

Chemical Name:but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide
CAS No.:675876-26-3
Molecular Formula:C₃₇H₃₃N₅O₇S
Molecular Weight:691.764
Hs Code.:

but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1<i>H</i>-pyrrol-2-yl]-methyl}-amide

Synonyms:but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide

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Chemical Property of but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide

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Technology Process of but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide

There total 4 articles about but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 15329-69-8
N-benzylmaleamic acid

: 88333-03-3,10340-91-7
Benzyl isocyanide

: Benzyl-[1-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-meth-(E)-ylidene]-amine

: 675876-26-3
but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide

Guidance literature:: In methanol; at 20 ℃; for 36h;
DOI:10.1021/jo030231z

Reference yield:

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 675876-26-3
but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / Et₃N; DMAP / CH₂Cl₂ / 15 h / 20 °C

2: TMOF / 20 °C

3: 80 percent / methanol / 36 h / 20 °C

With dmap; triethylamine; trimethyl orthoformate; In methanol; dichloromethane; 3: Ugi reaction;
DOI:10.1021/jo030231z

Reference yield:

: 54254-38-5
1-(2-nitrophenylsulfonyl)-1H-pyrrole-2-carboxaldehyde

: 675876-26-3
but-2-enedioic acid benzylamide benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide

Guidance literature:: Multi-step reaction with 2 steps

1: TMOF / 20 °C

2: 80 percent / methanol / 36 h / 20 °C

With trimethyl orthoformate; In methanol; 2: Ugi reaction;
DOI:10.1021/jo030231z