3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carboxamide

Base Information

• Chemical Name: 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carboxamide
• CAS No.: 1024005-21-7
• Molecular Formula: C₁₅H₁₃F₂N₃O
• Molecular Weight: 289.285

Synonyms:3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carboxamide

Chemical Property of 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carboxamide

Chemical Property:

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Technology Process of 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carboxamide

There total 1 articles about 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-dien-5-carboxylic acid (916591-87-2,916591-89-4,916591-88-3) → 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carboxamide (1024005-21-7)

Guidance literature:

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxylic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 35 ℃; for 3h;

With ammonia; In water; at 20 - 35 ℃; for 1h;

Reference yield: 95.0%

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carboxamide (1024005-21-7) → 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbonitrile (1024005-25-1)

Guidance literature:

With thionyl chloride; In 1,4-dioxane; at 0 ℃; for 5.16667h; Heating / reflux;

Reference yield: 49.0%

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carboxamide (1024005-21-7) → amino-5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-diene-3yl-methanethione (1024005-24-0)

Guidance literature:

With pyridine; phosphorous (V) sulfide; for 3h; Heating / reflux;

upstream raw materials:

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxylic acid

Downstream raw materials:

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbonitrile

amino-5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-diene-3yl-methanethione

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