2-prop-2-enyl-3a,4,5,6,7,7a-hexahydroisoindole-1,3-dione

Base Information

Chemical Name:2-prop-2-enyl-3a,4,5,6,7,7a-hexahydroisoindole-1,3-dione
CAS No.:68260-70-8
Molecular Formula:C11H15NO2
Molecular Weight:193.24
Hs Code.:
Mol file:68260-70-8.mol

Synonyms:2-Allyl-(3ar,7ac)-hexahydro-isoindol-1,3-dion;2-(prop-2-en-1-yl)hexahydro-1h-isoindole-1,3(2h)-dione;cis-2-allylhexahydroisoindole-1,3-dione;2-allyl-(3ar,7ac)-hexahydro-isoindole-1,3-dione;

Suppliers and Price of 2-prop-2-enyl-3a,4,5,6,7,7a-hexahydroisoindole-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-prop-2-enyl-3a,4,5,6,7,7a-hexahydroisoindole-1,3-dione

Chemical Property:

Vapor Pressure:3.24E-05mmHg at 25°C
Boiling Point:354.9°C at 760 mmHg
Flash Point:163.7°C
PSA：37.38000
Density:1.111g/cm³
LogP:1.28550

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-prop-2-enyl-3a,4,5,6,7,7a-hexahydroisoindole-1,3-dione

There total 4 articles about 2-prop-2-enyl-3a,4,5,6,7,7a-hexahydroisoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 610-09-3
(1R,2S)-cyclohexane-1,2-dicarboxylic acid

: 107-11-9,30551-89-4
1-amino-2-propene

: 68260-70-8
cis-2-allylhexahydroisoindole-1,3-dione

Guidance literature:: microwave irradiation;
DOI:10.1016/j.tet.2006.09.051

Reference yield:

: (1R,2S)-2-Allylcarbamoyl-cyclohexanecarboxylic acid

: 68260-70-8
cis-2-allylhexahydroisoindole-1,3-dione

Guidance literature:: With 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In toluene; for 2h; Heating;
DOI:10.1016/j.tet.2006.09.051

Reference yield:

: 13149-00-3
1,2-cis-cyclohexanedicarboxylic anhydride

: 68260-70-8
cis-2-allylhexahydroisoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 1 h / 20 °C

2: ZnCl₂; HMDS / toluene / 2 h / Heating

With 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In toluene;
DOI:10.1016/j.tet.2006.09.051