3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose

Base Information

Chemical Name:3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose
CAS No.:113808-24-5
Molecular Formula:C₃₅H₃₄O₆
Molecular Weight:550.651
Hs Code.:

Synonyms:3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose

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Chemical Property of 3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose

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Technology Process of 3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose

There total 10 articles about 3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 613-90-1
benzoyl cyanide

: 113808-23-4
5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-α-D-ribo-hexofuranose

: 113808-24-5
3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose

Guidance literature:: With triethylamine; In 1,4-dioxane; at 20 ℃; for 1h;

Reference yield:

: 7057-09-2
1,2-O-isopropylidene-5-deoxy-α-D-glucofuranose

: 113808-24-5
3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine / 24 h / 20 °C

2: 1)dimethyl sulfoxide/acetic anhydride, 2)sodium borohydride / 1)1.5h, 70 deg C, 2)1h, room temperature

3: 85 percent / triethylamine / dioxane / 1 h / 20 °C

With pyridine; sodium tetrahydroborate; acetic anhydride; dimethyl sulfoxide; triethylamine; In 1,4-dioxane;

Reference yield:

: 76-83-5
trityl chloride

: 113808-24-5
3-O-benzoyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-ribo-hexofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine / 24 h / 20 °C

2: 1)dimethyl sulfoxide/acetic anhydride, 2)sodium borohydride / 1)1.5h, 70 deg C, 2)1h, room temperature

3: 85 percent / triethylamine / dioxane / 1 h / 20 °C

With pyridine; sodium tetrahydroborate; acetic anhydride; dimethyl sulfoxide; triethylamine; In 1,4-dioxane;