(3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane

Base Information

Chemical Name:(3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane
CAS No.:220563-70-2
Molecular Formula:C₃₅H₃₈N₂O₅
Molecular Weight:566.697
Hs Code.:

Synonyms:(3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane

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Chemical Property of (3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane

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Technology Process of (3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane

There total 1 articles about (3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 208455-27-0
(3R,6S,9S)-1-aza-2-oxo-3-amino-3-benzyl-9-tert-butoxycarbonyl-bicyclo[4.3.0]nonane

: 220563-70-2
(3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane

Guidance literature:: With 2,6-dimethylpyridine; In tetrahydrofuran; at 0 ℃; for 7h;

Reference yield:

: 220563-70-2
(3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane

: 220719-80-2
(3S,6R,8aR)-6-Benzyl-6-(9H-fluoren-9-ylmethoxycarbonylamino)-5-oxo-octahydro-indolizine-3-carboxylic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 1.5h; Ambient temperature;

Reference yield:

: 220563-70-2
(3S,6S,9S)-1-aza-3-benzyl-9-tert-butyloxycarbonyl-3-(9'-fluorenylmethoxycarbonylamino)-2-oxobicyclo<4,3,0>nonane

: Ac-Phe-<(5,6)-bicyclic lactam>-GlyOMe

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂ / 1.5 h / Ambient temperature

With trifluoroacetic acid; In dichloromethane;