Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide

Base Information

Chemical Name:Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide
CAS No.:77663-97-9
Molecular Formula:BrH*C₁₆H₁₉NO₆S
Molecular Weight:434.308
Hs Code.:

Synonyms:Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide

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Chemical Property of Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide

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Technology Process of Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide

There total 3 articles about Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 77663-85-5
N-(3,4,5-Trimetoxythiobenzoyl)glutamic acid 5-methyl ester

: 77663-97-9
Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 2h; Ambient temperature;
DOI:10.1002/ardp.19813140204

Reference yield:

: 1499-55-4
L-glutamic acid 5-methyl ester

: 77663-97-9
Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / triethylamine / dimethylsulfoxide / 16 h / 50 °C

2: 82 percent / 10percent HBr / acetic acid / 2 h / Ambient temperature

With hydrogen bromide; triethylamine; In acetic acid; dimethyl sulfoxide;
DOI:10.1002/ardp.19813140204

Reference yield:

: 65322-86-3
Methyl 3,4,5-trimethoxydithiobenzoate

: 77663-97-9
Methyl 4,5-dihydro-5-oxo-2-(3,4,5-trimethoxyphenyl)-4-thiazolepropionate hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / triethylamine / dimethylsulfoxide / 16 h / 50 °C

2: 82 percent / 10percent HBr / acetic acid / 2 h / Ambient temperature

With hydrogen bromide; triethylamine; In acetic acid; dimethyl sulfoxide;
DOI:10.1002/ardp.19813140204