pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate

Base Information

Chemical Name:pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate
CAS No.:839719-66-3
Molecular Formula:C₂₉H₁₈F₅NO₅
Molecular Weight:555.458
Hs Code.:

Synonyms:pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate

Suppliers and Price of pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate

Chemical Property:

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Technology Process of pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate

There total 1 articles about pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14533-84-7
pentafluorophenyl trifloroacetate

: 178119-93-2
N_α-Fmoc-(4-hydroxy)-D-phenylglycine

: 839719-66-3
pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1021/jm049906w

Reference yield: 72.0%

: 114459-62-0
tri-Boc-spermine

: 839719-66-3
pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate

: 839720-47-7
(3-tert-butoxycarbonylamino-propyl)-[4-(tert-butoxycarbonyl-{3-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-2-(4-hydroxy-phenyl)-acetylamino]-propyl}-amino)-butyl]-carbamic acid tert-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jm049906w

Reference yield:

: 839719-66-3
pentafluorophenyl D-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-4-hydroxybenzeneethanoate

: 839720-48-8
[4-({3-[2-amino-2-(4-hydroxy-phenyl)-acetylamino]-propyl}-tert-butoxycarbonyl-amino)-butyl]-(3-tert-butoxycarbonylamino-propyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Et₃N / CH₂Cl₂ / 3 h / 20 °C

2: 90 percent / 1-octanethiol; DBU / tetrahydrofuran / 2 h / 20 °C

With Octanethiol; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm049906w