6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid

Base Information

• Chemical Name: 6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid
• CAS No.: 1313494-75-5
• Molecular Formula: C₁₉H₁₅NO₄
• Molecular Weight: 321.332
• Mol file: 1313494-75-5.mol

Synonyms:6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid

Chemical Property of 6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid

There total 1 articles about 6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

6-amino-2-naphthoic acid (116668-47-4) + benzyl chloroformate (501-53-1,94274-21-2) → 6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid (1313494-75-5)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; at 20 ℃; for 17h;

DOI:10.1002/pola.24737

Reference yield: 71.0%

6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid (1313494-75-5) + phenol (108-95-2,27073-41-2) → C25H19NO4 (1313494-76-6)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 17h;

DOI:10.1002/pola.24737

Reference yield:

6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid (1313494-75-5) + C20H34N2O11*H(1+) → C39H47N3O14

Guidance literature:

6-(((benzyloxy)carbonyl)amino)-2-naphthoic acid; With benzotriazol-1-ol; diisopropyl-carbodiimide; In dichloromethane; at 0 ℃; for 0.25h;

C₂₀H₃₄N₂O₁₁*H⁽¹⁺⁾; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

upstream raw materials:

6-amino-2-naphthoic acid

benzyl chloroformate

Downstream raw materials:

C₁₇H₁₃NO₂

C₂₄H₂₅NO₆

C₂₄H₂₇NO₅

C₂₅H₁₉NO₄