7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl

Base Information

Chemical Name:7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl
CAS No.:1278072-04-0
Molecular Formula:C₄₄H₃₈Br₂N₂O₂
Molecular Weight:786.606
Hs Code.:

Synonyms:7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl

Chemical Property:

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Technology Process of 7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl

There total 3 articles about 7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422969-71-8
C₄₄H₄₀N₂O₂

: 1278072-04-0
7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl

Guidance literature:: With N-Bromosuccinimide; acetic acid; In chloroform;
DOI:10.1166/jnn.2012.5886

Reference yield:

: 1422969-69-4
3-bromo-10-(4-(tert-butyl)phenyl)-10H-phenoxazine

: 1278072-04-0
7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: palladium diacetate; potassium carbonate; Tri(p-tolyl)phosphine / 1,2-dimethoxyethane; water

3: N-Bromosuccinimide; acetic acid / chloroform

With N-Bromosuccinimide; n-butyllithium; palladium diacetate; potassium carbonate; acetic acid; Tri(p-tolyl)phosphine; In tetrahydrofuran; 1,2-dimethoxyethane; chloroform; water; 2: Suzuki coupling;
DOI:10.1166/jnn.2012.5886

Reference yield:

: 1422969-69-4
3-bromo-10-(4-(tert-butyl)phenyl)-10H-phenoxazine

: 1422969-70-7
C₂₈H₃₂BNO₃

: 1278072-04-0
7,7'-dibromo-10,10'-bis-(4-tert-butyl-phenyl)-10H,10'H-[3,3']biphenothiazinyl

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; potassium carbonate; Tri(p-tolyl)phosphine / 1,2-dimethoxyethane; water

2: N-Bromosuccinimide; acetic acid / chloroform

With N-Bromosuccinimide; palladium diacetate; potassium carbonate; acetic acid; Tri(p-tolyl)phosphine; In 1,2-dimethoxyethane; chloroform; water; 1: Suzuki coupling;
DOI:10.1166/jnn.2012.5886