N-[⁽¹⁾-1-(2-bromo-6-chlorophenyl)-3-(trimethylsilyl)-2-propyn-1-ylidene]-2-(1-methylethyl)aniline

Base Information

• Chemical Name: N-[⁽¹⁾-1-(2-bromo-6-chlorophenyl)-3-(trimethylsilyl)-2-propyn-1-ylidene]-2-(1-methylethyl)aniline
• CAS No.: 1070870-35-7
• Molecular Formula: C₂₁H₂₃BrClNSi
• Molecular Weight: 432.863

Synonyms:N-[⁽¹⁾-1-(2-bromo-6-chlorophenyl)-3-(trimethylsilyl)-2-propyn-1-ylidene]-2-(1-methylethyl)aniline

Chemical Property of N-[⁽¹⁾-1-(2-bromo-6-chlorophenyl)-3-(trimethylsilyl)-2-propyn-1-ylidene]-2-(1-methylethyl)aniline

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Technology Process of N-[⁽¹⁾-1-(2-bromo-6-chlorophenyl)-3-(trimethylsilyl)-2-propyn-1-ylidene]-2-(1-methylethyl)aniline

There total 1 articles about N-[⁽¹⁾-1-(2-bromo-6-chlorophenyl)-3-(trimethylsilyl)-2-propyn-1-ylidene]-2-(1-methylethyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

2-bromo-6-chloro-N-[2-(1-methylethyl)phenyl]benzamide (1070870-34-6) + copper(I) (trimethylsilyl)acetylide (53210-13-2) → N-[(1)-1-(2-bromo-6-chlorophenyl)-3-(trimethylsilyl)-2-propyn-1-ylidene]-2-(1-methylethyl)aniline (1070870-35-7)

Guidance literature:

2-bromo-6-chloro-N-[2-(1-methylethyl)phenyl]benzamide; With 2-chloropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; for 0.416667h; Inert atmosphere;

copper(I) (trimethylsilyl)acetylide; In tetrahydrofuran; dichloromethane; at -78 - 0 ℃; for 0.25h;

Reference yield: 49.0%

N-[(1)-1-(2-bromo-6-chlorophenyl)-3-(trimethylsilyl)-2-propyn-1-ylidene]-2-(1-methylethyl)aniline (1070870-35-7) → 2-(2-bromo-6-chlorophenyl)-8-(1-methylethyl)quinoline (1070870-36-8)

Guidance literature:

With ammonium hexafluorophosphate; chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II); In toluene; at 115 ℃; for 19h;

upstream raw materials:

2-bromo-6-chloro-N-[2-(1-methylethyl)phenyl]benzamide

copper(I) (trimethylsilyl)acetylide

Downstream raw materials:

2-(2-bromo-6-chlorophenyl)-8-(1-methylethyl)quinoline

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