C₃₀H₄₃NO₃S₂

Base Information

• Chemical Name: C₃₀H₄₃NO₃S₂
• CAS No.: 1351657-13-0
• Molecular Formula: C₃₀H₄₃NO₃S₂
• Molecular Weight: 529.808

Synonyms:C₃₀H₄₃NO₃S₂

Chemical Property of C₃₀H₄₃NO₃S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₃NO₃S₂

There total 23 articles about C₃₀H₄₃NO₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

C33H47NO3S2 (1351657-12-9) → C30H43NO3S2 (1351657-13-0)

Guidance literature:

With hydrogenchloride; In methanol;

DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

C14H26O4 (1351656-96-6) → C30H43NO3S2 (1351657-13-0)

Guidance literature:

Multi-step reaction with 20 steps

1: diisobutylaluminium hydride / tetrahydrofuran

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

3: sodium hydride / tetrahydrofuran

4: diisobutylaluminium hydride / tetrahydrofuran

5: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

6: pyridine; tributylphosphine

7: dichloromethane

8: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

9: sodium periodate / methanol; water

10: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

11: sodium hydride / tetrahydrofuran

12: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

13: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

14: lithium diisopropyl amide / tetrahydrofuran

15: lithium aluminium tetrahydride / tetrahydrofuran

16: 1H-imidazole / dichloromethane

17: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

18: tetrabutyl ammonium fluoride / tetrahydrofuran

19: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

20: hydrogenchloride / methanol

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 2: Swern oxidation / 3: Horner-Emmons olefination / 5: Katsuki-Sharpless epoxidation / 10: Pummerer rearrangement / 11: Horner-Emmons olefination;

DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

(2R,4R)-2-Methyl-4-((4S,5R)-2,2,5-trimethyl-[1,3]dioxan-4-yl)-pentan-1-ol (80657-88-1) → C30H43NO3S2 (1351657-13-0)

Guidance literature:

Multi-step reaction with 19 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

2: sodium hydride / tetrahydrofuran

3: diisobutylaluminium hydride / tetrahydrofuran

4: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

5: pyridine; tributylphosphine

6: dichloromethane

7: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

8: sodium periodate / methanol; water

9: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

10: sodium hydride / tetrahydrofuran

11: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

12: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

13: lithium diisopropyl amide / tetrahydrofuran

14: lithium aluminium tetrahydride / tetrahydrofuran

15: 1H-imidazole / dichloromethane

16: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

17: tetrabutyl ammonium fluoride / tetrahydrofuran

18: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

19: hydrogenchloride / methanol

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 1: Swern oxidation / 2: Horner-Emmons olefination / 4: Katsuki-Sharpless epoxidation / 9: Pummerer rearrangement / 10: Horner-Emmons olefination;

DOI:10.1016/j.tetlet.2011.10.073

upstream raw materials:

(2R,4R)-2-Methyl-4-((4S,5R)-2,2,5-trimethyl-[1,3]dioxan-4-yl)-pentan-1-ol

C₁₄H₂₆O₄

C₁₅H₂₈O₃

C₁₅H₂₈O₄

Downstream raw materials:

C₃₆H₅₇NO₃S₂Si

C₃₆H₅₅NO₃S₂Si

C₃₈H₆₁NO₃S₂Si

C₃₈H₆₁NO₅S₂Si

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