Phosphoric acid dibenzyl ester cyclohexylmethyl ester

Base Information

• Chemical Name: Phosphoric acid dibenzyl ester cyclohexylmethyl ester
• CAS No.: 136025-57-5
• Molecular Formula: C₂₁H₂₇O₄P
• Molecular Weight: 374.417
• Mol file: 136025-57-5.mol

Synonyms:Phosphoric acid dibenzyl ester cyclohexylmethyl ester

Chemical Property of Phosphoric acid dibenzyl ester cyclohexylmethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Phosphoric acid dibenzyl ester cyclohexylmethyl ester

There total 2 articles about Phosphoric acid dibenzyl ester cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

Cyclohexylmethyl-phosphoramidic acid dibenzyl ester (136025-53-1) → Phosphoric acid dibenzyl ester cyclohexylmethyl ester (136025-57-5)

Guidance literature:

With isopentyl nitrite; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4039(00)79706-1

Reference yield:

dibenzyl hydrogen phosphite (538-60-3) → Phosphoric acid dibenzyl ester cyclohexylmethyl ester (136025-57-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 52 percent / CCl₄

2: 50 percent / isoamyl nitrite / CH₂Cl₂ / Ambient temperature

With isopentyl nitrite; In tetrachloromethane; dichloromethane;

DOI:10.1016/S0040-4039(00)79706-1

Reference yield: 97.0%

Phosphoric acid dibenzyl ester cyclohexylmethyl ester (136025-57-5) → cyclohexylmethyl 1-monophosphate (33026-79-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;

DOI:10.1016/S0040-4039(00)79706-1

upstream raw materials:

Cyclohexylmethyl-phosphoramidic acid dibenzyl ester

dibenzyl hydrogen phosphite

Downstream raw materials:

cyclohexylmethyl 1-monophosphate