(1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate

Base Information

Chemical Name:(1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate
CAS No.:120586-31-4
Molecular Formula:C₂₂H₂₄O₅
Molecular Weight:368.43
Hs Code.:

Synonyms:(1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate

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Chemical Property of (1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate

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Technology Process of (1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate

There total 8 articles about (1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53996-40-0
3,4-bis(benzoloxy)furan

: 120586-31-4
(1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: diethylaluminium chloride / CH₂Cl₂ / 120 h / -20 °C

2: 84 percent / PBr₃ / dimethylformamide / 0 °C

3: 95 percent / lithium aluminium hydride / diethyl ether / Ambient temperature

4: 45 percent / Raney Ni (W-2) / ethanol / Ambient temperature

5: Jones reagent / acetone / Ambient temperature

6: diethyl ether; methanol

With lithium aluminium tetrahydride; jones reagent; diethylaluminium chloride; phosphorus tribromide; Raney Ni (W-2); In methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 120586-29-0
<(1S,2S,3S,4S)-5,6-dibenzyloxy-3-(2-pyridylthio)-7-oxabicyclo<2.2.1>hept-5-en-2-yl>methanol

: 120586-31-4
(1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / Raney Ni (W-2) / ethanol / Ambient temperature

2: Jones reagent / acetone / Ambient temperature

3: diethyl ether; methanol

With jones reagent; Raney Ni (W-2); In methanol; diethyl ether; ethanol; acetone;

Reference yield:

: 120586-28-9
(1S,2R,3S,4S)-5,6-Bis-benzyloxy-3-(pyridin-2-ylsulfanyl)-7-oxa-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

: 120586-31-4
(1S,2R,4R,5S,6R)-methyl 5,6-dibenzyloxy-7-oxabicyclo<2.2.1>heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / lithium aluminium hydride / diethyl ether / Ambient temperature

2: 45 percent / Raney Ni (W-2) / ethanol / Ambient temperature

3: Jones reagent / acetone / Ambient temperature

4: diethyl ether; methanol

With lithium aluminium tetrahydride; jones reagent; Raney Ni (W-2); In methanol; diethyl ether; ethanol; acetone;