4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene

Base Information

Chemical Name:4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene
CAS No.:1358581-18-6
Molecular Formula:C₁₄H₁₁BrClFO
Molecular Weight:332.572
Hs Code.:

Synonyms:4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene

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Chemical Property of 4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene

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Technology Process of 4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene

There total 8 articles about 4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.4%

: 811-98-3
d⁽⁴⁾-methanol

: 1358581-17-5
4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-phenol

: 1358581-18-6
4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene

Guidance literature:: 4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-phenol; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; for 18.5h;

d⁽⁴⁾-methanol; In tetrahydrofuran;

Reference yield:

: 1358580-28-5
(5-bromo-2-chloro-phenyl)-(4-ethoxy-3-fluoro-phenyl)methanone

: 1358581-18-6
4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.5 h / 20 °C

2: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 3 h

3: boron tribromide / dichloromethane / 4 h / Cooling with ice

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18.5 h

With methanol; triethylsilane; sodium tetrahydroborate; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; boron tribromide; triphenylphosphine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1358580-30-9
(5-bromo-2-chloro-phenyl)-(4-ethoxy-3-fluoro-phenyl)methanol

: 1358581-18-6
4-[(5-bromo-2-chloro-phenyl)methyl]-2-fluoro-1-(trideuteriomethoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 3 h

2: boron tribromide / dichloromethane / 4 h / Cooling with ice

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18.5 h

With triethylsilane; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; boron tribromide; triphenylphosphine; In tetrahydrofuran; dichloromethane;