(3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate

Base Information

Chemical Name:(3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate
CAS No.:1258299-36-3
Molecular Formula:C₂₇H₃₇N₃O₅
Molecular Weight:483.608
Hs Code.:

Synonyms:(3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate

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Chemical Property of (3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate

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Technology Process of (3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate

There total 1 articles about (3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1258299-35-2
C₃₇H₄₉N₃O₈

: 1258299-36-3
(3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate

Guidance literature:: With water; sodium carbonate; In methanol; at 40 ℃; for 1h;
DOI:10.1016/j.bmcl.2010.08.096

Reference yield: 99.0%

: 1258299-36-3
(3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate

: 106-95-6
allyl bromide

: 1258299-37-4
(3S,4S)-tert-butyl 3-(allyloxy)-4-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)pyrrolidine-1-carboxylate

Guidance literature:: (3S,4S)-tert-butyl 3-((6-(benzyl(tert-butoxycarbonyl)amino)pyridin-2-yl)methyl)-4-hydroxypyrrolidine-1-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.25h;

allyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃;
DOI:10.1016/j.bmcl.2010.08.096